Analisis Kadar Residu Pestisida Asefat pada Biji Kakao dan Biji Cengkeh Menggunakan Kromatografi Gas

Abstract

Determination of acephate pesticide residues in cocoa and clove seeds using gas chromatography. Gas chromatography equipped with FPD detector, column DB5, H2 carrier gas with a flow rate of 75 kPa. Column temperature used 100 ° C-250 ° C, a temperature of 230 ° C injector and detector temperature of 250 ° C. From the results obtained in cocoa beans A 0.0144 mg / kg and cocoa B 0.0144 mg / kg, while the seed cloves A 0.0003 mg / kg and cloves B 0.0007 mg / kg, indicating this value does not exceed the maximum limits of pesticide residues that have been established by Regulation of the Minister of Agriculture No. 24 / Permentan / SR. 140/4/2011 of technical registration and licensing of pesticides that if the value of the ADI for humans ≤ 0015 mg / kg (equal to the estimated safe level of residue ≤ 1 ppm).